HAZOP Study for Batch Process

As you know the Hazard and Operability (HAZOP) is a structural and systematic examination of the complex process or system to identify and evaluate potential hazards and operability issues. It is commonly used in industries such as chemical, petrochemical, and nuclear process.

HAZOP can be applied to both continuous and batch processes, but there are some differences in how the studies are conducted to the nature of these processes. Below is the comparison between the continuous process and the batch Process.

SubjectContinuousBatch
Process DynamicsThe process operates continuously without interruption, The study focuses on the deviations from the normal operating. The process operates in a series of steps with intermittent periods of production.
Mode Normal, Start-up, and ShutdownMultiple phases/steps
Transient conditionLimit to only start-up, shutdown, and online mode changeAlways study the transient
Flexibility and VariabilityLimit to only some activities such as chemical loading More flexibility, especially Time-related guidewords
Time considerationLimit only 2 dimensions are (NO/LESS) and Extend (MORE).Many dimensions of Time-related deviation

From the above table, the main difference between the batch process and the continuous process is the process dynamics. The batch process will be discussed repeatedly in a series of steps. Hence, the workshop can become worse (discussion back and forth across the worksheet) if not well prepared.

Time-Related Guidewords of the Batch Operation

Below is an example of time-related guidewords that can be applied during the workshop, if relevant. However, it obviously be noticed those guidewords become more relevant when encompassed with human factors.

GuidewordInterpretation
Early/beforesomething errors and do something earlier than required.
Late/aftersomething errors and do something later than required.
Quickersomething errors and do something quicker than required.
Slowersomething errors and do something slower than required.
Repeated something errors and do something double.
Table of additional HAZOP Guidewords for the Batch HAZOP

Example

Below is an example of the Process Flow Diagram (PFD) of the Carbon Filter and Cation Filter in the Demineralized Water Package.

StageDescriptionService InletService OutletBackwash InletBackwash OutletRinse OutletVent
1Venting O
2Filling O
3Pre-Service RinseOO
4ServiceOO
5Back WashOO
6Final Rinse and DrainOOO

The HAZOP worksheet will look like this.

DeviationCause
No/Less FlowFailure and stuck closing of vent valve during the venting stage.
Failure and stuck closing of the serive inlet valve during Pre-Service Rinse
Failure and stuck closing of the service inlet valve during Rinse Outlet

The other way around is using the Failure Mode Effect Analysis (FMEA) study for 2 modes either open or closed failure mode during a review against all working steps.

Failure ModeSequenceConsequnce
Fail Close of Service InletVenting No safety issues as the system will understand it as a normal condition.
Filling Leading to No/Less flow of liquid supply to…
Pre-Service RinseLeading to No/Less flow of liquid supply to…
ServiceLeading to No/Less flow of liquid supply to…
Back WashNo safety issues as the system will understand it as a normal condition.
Final Rinse and DrainLeading to No/Less flow of liquid supply to…

In this way, all valves will be reviewed against all operation modes.